M&P Technologies, Inc.

4870 Lake Fjord Pass
Marietta, GA  30068

 

770-993-7397 Phone

770-993-7459 Fax
ASAP@MandPTechnologies.com

 

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Chemical Analysis Laboratories

The Chemical Analysis Laboratories (IRSL) is housed in the Research Center for Science and Technology at Clark Atlanta University.  The main goal of these laboratories is to carry out research involving the use of infrared spectroscopy, Raman spectroscopy and/or Nuclear Magnetic Resonance.

INFRARED SPECTROSCOPY
The main instrument for infrared spectroscopy in the IRSL is a Nicolet Magna 750 FT-IR spectrometer.  The main sample compartment of the instrument can be configured for Near-IR, Mid-IR or Far-IR work, such that spectra can be measured all the way from 1.1 mm to 200 mm (9,000 cm-1 to 50 cm-1), at a resolution of 0.125 cm-1.  This is achieved through the use of a combination of different sources, beamsplitters, and detectors.  An auxiliary sample compartment with a dedicated fast, liquid-nitrogen cooled infrared detector is typically dedicated to the in situ study of catalysts.  A Nicolet Nic-Plan microscope with a computer-controlled positioning stage is also coupled directly to the main interferometer.  In Table 1 are listed the techniques and capabilities which currently exist in the IRSL for infrared studies.  The ASTM methods which apply are outlined in E1252-94e1.  In addition, there are a wide variety of specific-compound methods outlined in ASTM methods which can be carried out easily using the equipment in the IRSL.

RAMAN SPECTROSCOPY
Two instruments are available in the IRSL for Raman Spectroscopy.  One instrument is a Nicolet Fourier transform Raman spectrometer (FT-Raman) which uses a long wavelength Nd-YAG laser for excitation.  This technique has the advantage that materials which fluoresce can be examined using Raman spectroscopy via this method.  The other instrument uses a shorter wavelength Ar+-ion laser for excitation, either 514 nm or 488 nm currently, although the other Ar+-ion laser wavelengths are available as well as a dye laser if appropriate filters are purchased.  A 0.5m Spex monochromator with CCD detector is available for use with the excitation source.  A macro chamber is available for normal samples as well as an Olympus microscope for micro-Raman studies.

NUCLEAR MAGNETIC RESONANCE
The NMR Laboratory is housed in the Research Center for Research and technology at Clark Atlanta Universities.  The NMR centers main function it to provide NMR services to the University and Industrial Communities.  In addition, the NMR laboratory provides for the training of students on the use on our NMR spectrometers.

    

    

    

Instruments / Capabilities

Capability / Sample Form
Method
Instruments
Solids/Powders/Fibers
  • KBr Pellet
  • Nujol Mull
  • Ambient Diffuse Reflectance
  • Controlled Environment Diffuse Reflectance
  • Attenuated Total Reflectance (ATR)
  • Micro-Reflectance
Nicolet Magna 750 FT-IR spectrometer
Polymers
  • Thin Film Transmission
  • ATR
  • Controlled Temperature ATR
  • External Reflectance
  • Micro-ATR
  • Micro-Reflectance
  • Micro-Transmission
Nicolet Magna 750 FT-IR spectrometer
Liquids
  • Thin Film Transmission
  • ATR
  • Controlled Temperature ATR
  • Micro-Reflectance
  • Micro-ATR
  • Micro-Transmission
Nicolet Magna 750 FT-IR spectrometer
Thin Films
  • Transmission
  • ATR
  • Controlled Temperature ATR
  • External Reflectance
  • Micro-Reflectance
  • Micro-ATR
  • Micro-Transmission
Nicolet Magna 750 FT-IR spectrometer
Gases
  • Transmission (10 cm gas cell)
  • Transmission (2.4m folded path, small volume gas cell)
Nicolet Magna 750 FT-IR spectrometer
Solids/Powders/Fibers
  • Solids/Powders/Fibers Standard Raman Scattering (Ar+ Ion and dye laser)
  • Micro Raman (Ar+ Ion and dye laser)
  • FT-Raman (Nd-YAG)
Nicolet Fourier transform Raman spectrometer with Nd-YAG laser 
Polymers
  • Polymers Standard Raman Scattering (Ar+ Ion and dye laser
  • Micro-Raman (Ar+ Ion and dye laser)
  • FT-Raman (Nd-YAG)
Nicolet Fourier transform Raman spectrometer with Nd-YAG laser 
Liquids
  • Standard Raman Scattering (Ar+ Ion and dye laser)
Nicolet Fourier transform Raman spectrometer with Nd-YAG laser 
Thin Films
  • Standard Raman Scattering (Ar+ Ion and dye laser) 
  • Micro Raman (Ar+ Ion and dye laser)
  • FT-Raman (Nd-YAG)
Nicolet Fourier transform Raman spectrometer with Nd-YAG laser 
Solution 80 MHz 1H and hetero-nuclear NMR 
  • User Defined 
  • ASTM E386-90(1995)
  • e1Double resonance
  • 2-D NMR
Bruker AC80 
Solution 250 MHz 1H and hetero-nuclear NMR 
  • User Defined
  • ASTM E386-90(1995)
  • e1Double resonance
  • 2-D NMR
Bruker WM250 
Solution 400 MHz 1H and hetero-nuclear NMR
  • User Defined
  • ASTM E386-90(1995)
  • e1Double resonance
  • 2-D NMR
Bruker ARX400 
Solid State 50 MHz NMR 13C and other hetero-nuclear NMR
  • User Defined
  • Magic Angle Spinning 
Bruker MSL200 
 

 

 

Contact us at: 


4870 Lake Fjord Pass 
Marietta, GA 30068 

770-993-7397 Phone 
770-993-7459 Fax 

or 

ASAP@MandPTechnologies.com

 

 

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